Dynamic phase diagram of soft nanocolloids

Author(s)
Sudipta Gupta, Manuel Camargo, Joerg Stellbrink, Juergen Allgaier, Aurel Radulescu, Peter Lindner, Emanuela Zaccarelli, Christos N. Likos, Dieter Richter
Abstract

We present a comprehensive experimental and theoretical study covering micro-, meso-and macroscopic length and time scales, which enables us to establish a generalized view in terms of structure-property relationship and equilibrium dynamics of soft colloids. We introduce a new, tunable block copolymer model system, which allows us to vary the aggregation number, and consequently its softness, by changing the solvophobic-to-solvophilic block ratio (m: n) over two orders of magnitude. Based on a simple and general coarse-grained model of the colloidal interaction potential, we verify the significance of interaction length sigma(int) governing both structural and dynamic properties. We put forward a quantitative comparison between theory and experiment without adjustable parameters, covering a broad range of experimental polymer volume fractions (0.001 <= phi <= 0.5) and regimes from ultra-soft star-like to hard sphere-like particles, that finally results in the dynamic phase diagram of soft colloids. In particular, we find throughout the concentration domain a strong correlation between mesoscopic diffusion and macroscopic viscosity, irrespective of softness, manifested in data collapse on master curves using the interaction length sigma(int) as the only relevant parameter. A clear reentrance in the glass transition at high aggregation numbers is found, recovering the predicted hard-sphere (HS) value in the hard-sphere like limit. Finally, the excellent agreement between our new experimental systems with different but already established model systems shows the relevance of block copolymer micelles as a versatile realization of soft colloids and the general validity of a coarse-grained approach for the description of the structure and dynamics of soft colloids.

Organisation(s)
Computational and Soft Matter Physics
External organisation(s)
Institut Laue-Langevin (ILL), Sapienza University of Rome, Forschungszentrum Jülich, Oak Ridge National Laboratory , Universidad Antonio Nariño, Technische Universität München
Journal
Nanoscale
Volume
7
Pages
13924-13934
No. of pages
11
ISSN
2040-3364
DOI
https://doi.org/10.1039/c5nr03702f
Publication date
2015
Peer reviewed
Yes
Austrian Fields of Science 2012
103018 Materials physics, 103029 Statistical physics, 210004 Nanomaterials
Keywords
ASJC Scopus subject areas
General Materials Science
Portal url
https://ucrisportal.univie.ac.at/en/publications/1c498d65-30e2-4c1c-9258-aec715414e28